Synonym:
Chlorotrimethylsilane,
N,O-Bis(trimethylsilyl)acetamide,
TSIM,
Trimethylchlorosilane,
Trimethylsilyl chloride,
Trimethylsilylimidazole
Properties:
Related Categories |
Analytical Reagents,
Analytical/Chromatography,
Derivatization Reagents,
Derivatization Reagents GC,
Reagents for Silylation,
|
grade
|
for GC/MS (SIM)
|
description
|
3:2:3 (SYLON BTZ)
|
packaging
|
pkg of 20 × 1 mL
|
concentration
|
(3:2:3)
|
derivatization reagent for
|
Acylations
|
|
Silylations
|
Description:
Application
It was used during derivatization of the sample for multi-mycotoxin analysis using gas chromatography (GC) coupled to triple quadrupole instrument (QqQ). It was also used as derivatizing reagent in the determination of trichothecenes, patulin and zearalenone using GC-MS/MS.
General description
Reagent mixture consisting of BSA+TMCS+TMSI when heated with pyridine and steroid at 60°C for 12 hours, converts 11- and the tertiary 17-hydroxyl groups to trimethylsilyl ethers.
Safety:
Hazard statements
H225-H302-H314-H335
Precautionary statements
P210-P261-P280-P305 + P351 + P338-P310
Supplemental Hazard Statements
Corrosive to the respiratory tract., Reacts violently with water.
RIDADR
UN 2924 8(3) / PGII